| Titel: | NEXAFS Spectra in Fluorescence and Transmission Mode of Organo-Sulfur Compounds with varying Sulfur Strand Length |
| Autoren: |
Skudler, Konstantin, Physikalisch-Technische Bundesanstalt (PTB), Fachbereich 7.2, Röntgenmesstechnik mit Synchrotronstrahlung, ORCID: 0009-0003-3981-5709 Müller, Matthias, Physikalisch-Technische Bundesanstalt (PTB), Fachbereich 7.2, Röntgenmesstechnik mit Synchrotronstrahlung, ORCID: 0000-0003-0115-7854 |
| Beitragende: | HostingInstitution: Physikalisch-Technische Bundesanstalt (PTB), ISNI: 0000 0001 2186 1887 |
| Sprache: | en |
| DOI: | 10.7795/720.20241009 |
| Art der Ressource: | Dataset / Measurement Data |
| Herausgeber: | Physikalisch-Technische Bundesanstalt (PTB) |
| Rechte: |
https://creativecommons.org/licenses/by/4.0/ CC-BY 4.0 International |
| Beziehungen: | IsDocumentedBy: DOI https://doi.org/10.1039/D4JA00232F IsSourceOf: DOI https://doi.org/10.1039/D3CP02285D |
| Daten: |
Verfügbar: 2024-10-09 |
| Klassifikationen: | INSPEC A30 Atomic and molecular physics |
| Datei: |
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MD5 Prüfsumme: de1410f166f23b003ee980e26848f6af SHA256 Prüfsumme: 057e0418aa753dd40fa61eed28baf55d873174f4fc968841e3b7b08d3fabf368 |
| Schlagworte | X-ray spectrometry ; X-ray spectroscopy ; NEXAFS ; XAFS ; organo-sulfur ; sulfur strand length |
| Zusammenfassung: | This dataset includes NEXAFS spectra of organo-sulfur compounds with varying sulfur strand length from 1 to 3. The NEXAFS spectra were taken in fluorescence and transmission mode. All of the spectra have been taken at the FCM beamline in the PTB laboratory at BESSY II using Si (111) crystals. All experimental setup details are described in the manuscript "Self-Absorption Correction of NEXAFS Spectra for Intermediate Sample Thicknesses applied to Organo-Sulfur Model Compounds". In this manuscript, the data have been analyzed regarding the self-absorption effect, except for the DMDS data because of a leakage of the respective cell. The data from 2022 also appear in "NEXAFS spectra of model sulfide chains: implications for sulfur networks obtained from inverse vulcanization", yet without the self-absorption correction applied. In this manuscript, the spectroscopic signature of the organo-sulfur compounds was analyzed in detail. |
| Anderes: | We acknowledge funding by the German Research Foundation (DFG) through the Priority Programme “Polymer-based Batteries” (SPP 2248) under the projects CH 2376/2-1, MU 4632/1-1, WA 1687/12-1, MU 4632/1-2, SO 1213/17-2 and WA 1687/12-2. |
| Förderung: | Deutsche Forschungsgemeinschaft (DFG), ISNI: 0000 0001 2096 9829, Grant Title: Novel Li-S batteries with dual redox couples: design, synthesis, in operando X-ray studies and theoretical modelling, Grant Number: SPP 2248 |